1QP5
BASE-PAIRING SHIFT IN A DODECAMER CONTAINING A (CA)N TRACT
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 258 |
Detector technology | AREA DETECTOR |
Detector | SIEMENS |
Spacegroup name | H 3 |
Unit cell lengths | 65.900, 65.900, 47.100 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 15.000 - 2.600 |
R-factor | 0.161 |
Data reduction software | X-GEN |
Data scaling software | X-GEN |
Phasing software | ULTIMA |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 15.000 |
High resolution limit [Å] | 2.600 |
Rmerge | 0.062 |
Number of reflections | 1603 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 277 | WATER, SPERMINE, CACODYLATE, MAGNESIUM ACETATE, pH 6.0, VAPOR DIFFUSION at 277 K |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | SPERMINE | ||
2 | 1 | 2 | CACODYLATE | ||
3 | 1 | 3 | MAGNESIUM ACETATE |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | cacodylate | 50 (mM) | |
2 | 1 | drop | dodecamer duplex | 1 (mM) | |
3 | 1 | drop | spermine tetrachloride | 1.2 (mM) | |
4 | 1 | drop | magnesium acetate | 16 (mM) | |
5 | 1 | drop | 2,4-methypentanediol | 45 (%) |