1QNY
X-ray refinement of D2O soaked crystal of concanavalin A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 293 |
| Detector technology | IMAGE PLATE |
| Detector | R-AXIS II |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 89.110, 87.580, 63.260 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 33.700 - 1.800 |
| R-factor | 0.168 |
| Rwork | 0.168 |
| R-free | 0.19800 |
| Structure solution method | OTHER |
| RMSD bond length | 0.007 |
| RMSD bond angle | 24.960 * |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 33.700 | 1.760 |
| High resolution limit [Å] | 1.700 | 1.700 |
| Rmerge | 0.071 | 0.248 |
| Number of reflections | 24110 | 1129 * |
| Completeness [%] | 88.1 | 42.1 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | 6.5 | Greer, J., (1970) J. Mol. Biol., 48, 365. * |
