1QJC
Phosphopantetheine Adenylyltransferase from Escherichia coli in complex with 4'-phosphopantetheine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Spacegroup name | I 2 3 |
Unit cell lengths | 135.331, 135.331, 135.331 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 67.670 - 1.630 |
R-factor | 0.216 |
Rwork | 0.216 |
R-free | 0.24700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1b6t |
RMSD bond length | 0.005 |
RMSD bond angle | 1.100 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.000 | 1.910 |
High resolution limit [Å] | 1.800 | 1.800 |
Rmerge | 0.044 | 0.409 |
Number of reflections | 33838 | |
<I/σ(I)> | 44.2 | |
Completeness [%] | 86.3 | 51.5 |
Redundancy | 20.02 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5 | pH 5.00 |