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1QJB

14-3-3 ZETA/PHOSPHOPEPTIDE COMPLEX (MODE 1)

Replaces:  14PS
Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSRS BEAMLINE PX7.2
Synchrotron siteSRS
BeamlinePX7.2
Temperature [K]100
Detector technologyIMAGE PLATE
DetectorMARRESEARCH
Spacegroup nameP 21 21 21
Unit cell lengths68.350, 71.980, 131.000
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution15.000 - 2.000
R-factor0.21

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Rwork0.210
R-free0.28800
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)14-3-3 ZETA
RMSD bond length0.012
RMSD bond angle0.033
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareREFMAC
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]15.0002.090
High resolution limit [Å]2.0002.000
Rmerge0.0590.320
Number of reflections37059
<I/σ(I)>13.32.1
Completeness [%]83.541.6
Redundancy2
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

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6.24

*

used to seeding

*

Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirMES100 (mM)
21reservoir20 (mM)
31reservoirisopropanol15-17 (%)
41reservoirPEG400012 (%)

217705

PDB entries from 2024-03-27

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