1QIO
SPECIFIC CHEMICAL AND STRUCTURAL DAMAGE CAUSED BY INTENSE SYNCHROTRON RADIATION TO HEN EGG WHITE LYSOZYME
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-4 |
Synchrotron site | ESRF |
Beamline | ID14-4 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1999-05-15 |
Detector | ADSC QUANTUM 4 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 76.929, 76.929, 37.207 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 1.200 |
R-factor | 0.141 * |
R-free | 0.18700 * |
Structure solution method | OTHER |
Starting model (for MR) | 194l |
RMSD bond length | 0.013 * |
RMSD bond angle | 0.031 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.000 | 1.240 |
High resolution limit [Å] | 1.200 | 1.200 |
Rmerge | 0.061 * | 0.176 * |
Number of reflections | 34095 | |
<I/σ(I)> | 23.7 | 4.3 |
Completeness [%] | 95.3 | 69.2 |
Redundancy | 4.11 | 2.89 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.7 | CRYSTALLIZED FROM 2-6% NACL, 0.2 M SODIUM ACETATE PH 4.7. |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | 2-6 (%) | ||
2 | 1 | 1 | Na acetate | 0.2 (M) |