1QGR
STRUCTURE OF IMPORTIN BETA BOUND TO THE IBB DOMAIN OF IMPORTIN ALPHA (II CRYSTAL FORM, GROWN AT LOW PH)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-3 |
Synchrotron site | ESRF |
Beamline | ID14-3 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 1998-07-15 |
Detector | MARRESEARCH |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.896, 101.167, 83.831 |
Unit cell angles | 90.00, 87.86, 90.00 |
Refinement procedure
Resolution | 40.000 - 2.300 |
R-factor | 0.235 * |
Rwork | 0.235 |
R-free | 0.28500 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB IDCODE 1QGK |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (0.4) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 2.370 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.089 | 0.380 |
Number of reflections | 46295 | |
<I/σ(I)> | 13.7 | 2 |
Completeness [%] | 98.5 | 98.5 |
Redundancy | 7.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Batch method * | 3.9 | pH 3.9 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | PEG8000 | 16-20 (%) | |
2 | 1 | 1 | potassium phosphate | 50 (mM) | |
3 | 1 | 1 | beta-mercaptoethanol | 10 (mM) | |
4 | 1 | 1 | sodium iodide | 5 (mM) | |
5 | 1 | 1 | protain | 50 (mg/ml) |