1QCY
THE CRYSTAL STRUCTURE OF THE I-DOMAIN OF HUMAN INTEGRIN ALPHA1BETA1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-09-10 |
Detector | RIGAKU RAXIS IIC |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 74.457, 81.858, 37.316 |
Unit cell angles | 90.00, 90.78, 90.00 |
Refinement procedure
Resolution | 500.000 - 2.300 |
Rwork | 0.200 |
R-free | 0.25800 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.200 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 500.000 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.058 | |
Number of reflections | 9471 | |
Completeness [%] | 94.8 | 90.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 8.5 | 298 | PEG 4000, Na-acetate, glycerol, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 298.0K |