1QBE

BACTERIOPHAGE Q BETA CAPSID

Experimental procedure

Spacegroup name	C 2 2 21
Unit cell lengths	477.800, 295.200, 477.800
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	15.000 - 3.500
R-factor	0.344 *
Rwork	0.304
RMSD bond length	0.009
RMSD bond angle	25.200 *
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	40.000 *
High resolution limit [Å]	3.500 *
Rmerge	0.201 *
Total number of observations	800000 *
Number of reflections	333576 *
Completeness [%]	80.5 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	7.4 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	PEG2000	10 (%)
2	1	drop	ammonium sulfate	0.3-0.45 (M)
3	1	drop	lithium chloride	0-0.2 (M)
4	1	drop	HEPES	5 (mg/ml)
5	1	reservoir	sodium chloride	0.4 (M)
6	1	reservoir	Tris	50 (mM)