1Q8B
Structural Genomics, protein YJCS
Experimental procedure
| Experimental method | MAD |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 19-ID |
| Synchrotron site | APS |
| Beamline | 19-ID |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2003-06-03 |
| Detector | SBC-2 |
| Wavelength(s) | 0.9795, 0.9797, 0.94656 |
| Spacegroup name | H 3 2 |
| Unit cell lengths | 71.095, 71.095, 149.210 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 31.900 - 1.900 |
| R-factor | 0.207 |
| Rwork | 0.207 |
| R-free | 0.25700 |
| Structure solution method | MAD |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.200 |
| Data scaling software | HKL-2000 |
| Phasing software | CNS |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 1.970 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Rmerge | 0.127 | 0.456 |
| Number of reflections | 10996 | |
| <I/σ(I)> | 30.54 | 3.76 |
| Completeness [%] | 93.5 | 96.1 |
| Redundancy | 13.04 | 6.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 |
