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1Q4R

Gene Product of At3g17210 from Arabidopsis Thaliana

Experimental procedure
Experimental methodMAD
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 14-ID-B
Synchrotron siteAPS
Beamline14-ID-B
Temperature [K]90
Detector technologyCCD
Collection date2003-06-26
DetectorMARRESEARCH
Wavelength(s)0.979
Spacegroup nameP 62
Unit cell lengths55.468, 55.468, 57.673
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution20.000 - 1.900
R-factor0.18469
Rwork0.182
R-free0.23200

*

Structure solution methodMAD
RMSD bond length0.020
RMSD bond angle1.861
Data scaling softwareSCALEPACK
Phasing softwareSOLVE (RESOLVE)
Refinement softwareREFMAC (5.1.24)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0001.970
High resolution limit [Å]1.9001.900
Rmerge0.0420.274

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Total number of observations75176

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Number of reflections14162

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<I/σ(I)>35.62.06
Completeness [%]93.5

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52.6

*

Redundancy5.2

*

2.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP7

*

297Sodium MES, Sodium citrate, MEthyl Ether PEG 5000, pH 6.0, VAPOR DIFFUSION, HANGING DROP, temperature 297K
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirmPEG500030 (%(w/v))
21reservoirsodium cirtate120 (mM)
31reservoirsodium HEPES100 (mM)pH6.0
41drop100 (mM)
51dropsodium HEPES10 (mM)pH7.0
61dropprotein14 (mg/ml)

217705

PDB entries from 2024-03-27

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