1Q13
Crystal structure of rabbit 20alpha hyroxysteroid dehydrogenase in ternary complex with NADP and testosterone
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 200 |
Detector technology | IMAGE PLATE |
Collection date | 2002-07-07 |
Detector | RIGAKU RAXIS IIC |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 57.210, 84.046, 66.249 |
Unit cell angles | 90.00, 91.17, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.080 |
R-factor | 0.22918 |
Rwork | 0.226 |
R-free | 0.28008 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.025 |
RMSD bond angle | 2.013 |
Data scaling software | XDS |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 5.060 | 2.150 |
High resolution limit [Å] | 2.080 | 2.100 |
Number of reflections | 37115 | |
Completeness [%] | 59 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | PEG4000, ammonium sulfate, pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |