1PZB
THE CRYSTAL STRUCTURES OF REDUCED PSEUDOAZURIN FROM ALCALIGENES FAECALIS S-6 AT TWO PH VALUES
Experimental procedure
Spacegroup name | P 65 |
Unit cell lengths | 49.950, 49.950, 98.500 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 1.800 |
R-factor | 0.177 |
RMSD bond length | 0.017 * |
RMSD bond angle | 3.200 * |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.800 * |
Rmerge | 0.050 * |
Total number of observations | 97396 * |
Number of reflections | 12660 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 8 * | Petratos, K., (1987) FEBS Lett., 218, 209. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 1.5 (%) | |
2 | 1 | drop | ammonium sulfate | 1.5 (M) | |
3 | 1 | drop | potassium phosphate | 50 (mM) | |
4 | 1 | reservoir | ammonium sulfate | 3.0 (M) |