1PXU
Crystal structure of chicken NtA from a eukaryotic source at 2.2A resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE BW7B |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | BW7B |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2002-01-01 |
Detector | MARRESEARCH |
Wavelength(s) | 0.8795 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 86.685, 50.401, 54.571 |
Unit cell angles | 90.00, 118.93, 90.00 |
Refinement procedure
Resolution | 28.030 - 2.200 |
R-factor | 0.197 |
Rwork | 0.197 |
R-free | 0.23300 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1jb3 |
RMSD bond length | 0.005 |
RMSD bond angle | 1.300 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | CNS (1.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 28.000 |
High resolution limit [Å] | 2.200 |
Number of reflections | 10565 |
Redundancy | 2.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.1 | 292 | peg 8000, pH 6.1, VAPOR DIFFUSION, HANGING DROP, temperature 292K |