1PUE
PU.1 ETS DOMAIN-DNA COMPLEX
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LURE BEAMLINE D41A |
Synchrotron site | LURE |
Beamline | D41A |
Temperature [K] | 130 |
Detector technology | AREA DETECTOR |
Collection date | 1994-01-21 |
Detector | UCSD MARK III |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 89.100, 101.900, 55.600 |
Unit cell angles | 90.00, 111.20, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.100 |
R-factor | 0.225 |
Rwork | 0.225 |
R-free | 0.28700 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.630 |
Data reduction software | MOSFLM |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | |
Rmerge | 0.033 |
Redundancy | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 6.5 | 19 * | Pio, F., (1995) J.Biol.Chem., 270, 24258. * |
1 | unknown * | 6.5 | 19 * | Pio, F., (1995) J.Biol.Chem., 270, 24258. * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | sodium cacodylate | 100 (mM) | |
2 | 1 | 1 | PEG600 | 3-10 (%) | |
3 | 1 | 1 | zinc acetate | 200 (mM) |