1PTK

STUDIES ON THE INHIBITORY ACTION OF MERCURY UPON PROTEINASE K

Experimental procedure

Spacegroup name	P 43 21 2
Unit cell lengths	68.360, 68.360, 108.410
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.400
R-factor	0.126
RMSD bond length	0.006
RMSD bond angle	1.400
Refinement software	TNT

Data quality characteristics

	Overall
Low resolution limit [Å]	8.000 *
High resolution limit [Å]	2.400 *
Rmerge	0.041 *
Number of reflections	8602 *
Completeness [%]	81.0 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, sitting drop *	7.5 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	enzyme	5 (%(w/v))
2	1	drop	Tris-HAc	50 (mM)
3	1	drop		5 (mM)
4	1	reservoir		0.8 (M)
5	1	reservoir	Tris-HAc	50 (mM)