1PTG

PHOSPHATIDYLINOSITOL-SPECIFIC PHOSPHOLIPASE C IN COMPLEX WITH MYO-INOSITOL

Experimental procedure

Detector technology	AREA DETECTOR
Collection date	1994
Detector	SIEMENS
Spacegroup name	P 21 21 21
Unit cell lengths	45.200, 45.600, 160.800
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	8.000 - 2.600
R-factor	0.195
Rwork	0.195
R-free	0.27400
Structure solution method	MIR
RMSD bond length	0.008
RMSD bond angle	1.600
Data reduction software	XDS
Phasing software	X-PLOR (3.1)
Refinement software	X-PLOR (3.1)

Data quality characteristics

	Overall
Low resolution limit [Å]	20.000
High resolution limit [Å]	2.500
Rmerge	0.045
Number of reflections	10300
Completeness [%]	78.0
Redundancy	3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1