1PPO

DETERMINATION OF THE STRUCTURE OF PAPAYA PROTEASE OMEGA

Experimental procedure

Spacegroup name	P 31 1 2
Unit cell lengths	74.110, 74.110, 77.810
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	10.000 * - 1.800
R-factor	0.155
RMSD bond length	0.025
RMSD bond angle	0.050
Refinement software	RESTRAIN

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	9999.000 *
High resolution limit [Å]	1.800 *	1.800 *
Rmerge	0.111 *	0.334 *
Completeness [%]	83.0 *	50 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	1.8 (%)
2	1	drop	Tris-HCl	50 (mM)
3	1	drop	sodium chloride	250 (mM)
4	1	reservoir	ethanol	82 (%)
5	1	reservoir	sodium chloride	182 (mM)