1PPN
STRUCTURE OF MONOCLINIC PAPAIN AT 1.60 ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 1 21 1 |
Unit cell lengths | 65.700, 50.700, 31.500 |
Unit cell angles | 90.00, 98.40, 90.00 |
Refinement procedure
Resolution | 10.000 - 1.600 |
R-factor | 0.1596 * |
Rwork | 0.160 |
RMSD bond length | 0.022 |
RMSD bond angle | 0.049 |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
High resolution limit [Å] | 1.600 * |
Completeness [%] | 93.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 5 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | 1 | papain | 1.3 (%) | |
2 | 1 | 1 | 25 (mM) | ||
3 | 1 | 1 | methanol | 25 (%(v/v)) | |
4 | 1 | 1 | sodium acetate | 0.1 (M) | |
5 | 1 | 2 | methanol | 67 (%(v/v)) |