1PPL
CRYSTALLOGRAPHIC ANALYSIS OF TRANSITION-STATE MIMICS BOUND TO PENICILLOPEPSIN: PHOSPHORUS-CONTAINING PEPTIDE ANALOGUES
Experimental procedure
Spacegroup name | C 1 2 1 |
Unit cell lengths | 97.500, 46.460, 65.930 |
Unit cell angles | 90.00, 115.20, 90.00 |
Refinement procedure
Resolution | 8.000 * - 1.700 |
R-factor | 0.148 |
Rwork | 0.148 |
RMSD bond length | 0.024 |
RMSD bond angle | 0.047 * |
Phasing software | X-PLOR |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 60.000 * |
High resolution limit [Å] | 1.700 * |
Rmerge | 0.060 * |
Total number of observations | 88917 * |
Number of reflections | 26533 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 4.4 * | 18-22 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | complex | 10 (mg/ml) | |
2 | 1 | drop | ammonium sulfate | 34-40 (%sat) | |
3 | 1 | drop | 0.1 (M) |