1PP2
THE REFINED CRYSTAL STRUCTURE OF DIMERIC PHOSPHOLIPASE A2 AT 2.5 ANGSTROMS. ACCESS TO A SHIELDED CATALYTIC CENTER
Experimental procedure
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 53.400, 100.200, 48.600 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | ? - 2.500 |
| R-factor | 0.178 |
| RMSD bond length | 0.028 |
| RMSD bond angle | 4.000 |
| Refinement software | PROLSQ |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | Microdialysis * | 7.2 * | 4 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | 100 (mM) | ||
| 2 | 1 | 1 | Tris-HCl | 10 (mM) | |
| 3 | 1 | 1 | phospholipase A2 solution | ||
| 4 | 1 | 1 | 0.1 (mM) | ||
| 5 | 1 | 2 | 10 (mM) | ||
| 6 | 1 | 2 | 0.1 (mM) |
