1POY
SPERMIDINE/PUTRESCINE-BINDING PROTEIN COMPLEXED WITH SPERMIDINE (DIMER FORM)
Experimental procedure
Detector technology | IMAGE PLATE |
Collection date | 1993-02-01 |
Detector | MACSCIENCE |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 145.300, 69.100, 72.500 |
Unit cell angles | 90.00, 107.60, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.500 |
R-factor | 0.199 |
Rwork | 0.199 |
R-free | 0.28000 |
RMSD bond length | 0.016 |
RMSD bond angle | 1.980 * |
Data reduction software | WELMS |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 300.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.068 * |
Number of reflections | 38903 |
Completeness [%] | 81.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * |