1POE
STRUCTURES OF FREE AND INHIBITED HUMAN SECRETORY PHOSPHOLIPASE A2 FROM INFLAMMATORY EXUDATE
Experimental procedure
Spacegroup name | P 43 21 2 |
Unit cell lengths | 76.300, 76.300, 115.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | ? - 2.100 |
R-factor | 0.196 |
Rwork | 0.196 |
RMSD bond length | 0.016 |
RMSD bond angle | 2.200 |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion * | 7.4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 10 (mg/ml) | |
2 | 1 | drop | 10 (mM) | ||
3 | 1 | drop | Tris-HCl | 0.1 (M) | |
4 | 1 | drop | 2.25 (M) | ||
5 | 1 | reservoir | 4.5 (M) | ||
6 | 1 | reservoir | Tris-HCl | 0.1 (M) |