1PML

KRINGLE-KRINGLE INTERACTIONS IN MULTIMER KRINGLE STRUCTURES

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	54.800, 63.580, 46.580
Unit cell angles	90.00, 106.70, 90.00

Refinement procedure

Resolution	8.000 - 2.380
R-factor	0.145
RMSD bond length	0.015
RMSD bond angle	0.054 *
Refinement software	PROFFT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.380 *	2.380 *
Rmerge	0.070 *
Total number of observations	30076 *
Number of reflections	11621 *	1101 *
Completeness [%]	91.0 *	52 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion *	8 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	4 (mg/ml)
2	1	reservoir	ammonium chloride	7 (%sat)
3	1	reservoir	ammonium bicarbonate	50 (mM)