1PMK

KRINGLE-KRINGLE INTERACTIONS IN MULTIMER KRINGLE STRUCTURES

Experimental procedure

Spacegroup name	P 1 21 1
Unit cell lengths	32.730, 49.090, 46.150
Unit cell angles	90.00, 100.60, 90.00

Refinement procedure

Resolution	7.000 - 2.250
R-factor	0.165
RMSD bond length	0.015
RMSD bond angle	0.046 *
Refinement software	PROFFT

Data quality characteristics

	Overall	Outer shell
High resolution limit [Å]	2.250 *	2.250 *
Number of reflections	4328 *
Completeness [%]	62.0 *	39 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	Vapor diffusion, hanging drop *	6.2 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	drop	protein	10 (mg/ml)
2	1	reservoir	ammonium sulfate	0.1 (M)
3	1	reservoir	PEG8000	35 (%)
4	1	reservoir	n-butanol	0.8 (%)