1PKY
PYRUVATE KINASE FROM E. COLI IN THE T-STATE
Experimental procedure
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Collection date | 1994-10-20 |
Detector | MARRESEARCH |
Wavelength(s) | 0.92 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.911, 129.577, 241.370 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.000 - 2.500 |
R-factor | 0.203 |
R-free | 0.30500 |
RMSD bond length | 0.016 |
RMSD bond angle | 0.035 |
Data reduction software | DENZO |
Refinement software | PROLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 10.000 |
High resolution limit [Å] | 2.500 |
Rmerge | 0.088 |
Total number of observations | 540887 * |
Number of reflections | 77917 |
Completeness [%] | 99.9 |
Redundancy | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.2 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 16 (%(w/v)) | |
2 | 1 | reservoir | 10 (mM) | ||
3 | 1 | reservoir | 10 (mM) | ||
4 | 1 | reservoir | MES/NaOH | 100 (mM) |