1PHR

THE CRYSTAL STRUCTURE OF A LOW MOLECULAR PHOSPHOTYROSINE PROTEIN PHOSPHATASE

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	46.300, 62.200, 62.700
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	6.000 - 2.100
R-factor	0.156 *
Rwork	0.167
R-free	0.20800 *
RMSD bond length	0.012 *
RMSD bond angle	2.600 *
Phasing software	X-PLOR
Refinement software	X-PLOR

Data quality characteristics

	Overall
High resolution limit [Å]	2.100 *
Rmerge	0.064 *
Number of reflections	9896 *
Completeness [%]	90.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	5.5 *		used as seeds *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	ammonium sulfate	40 (%)
2	1	1	DTT	10 (mM)
3	1	1	acetate	100 (mM)