1PHB

INHIBITOR-INDUCED CONFORMATIONAL CHANGE IN CYTOCHROME P450-CAM

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	108.670, 103.900, 36.380
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 2.100 *
R-factor	0.19
RMSD bond length	0.018 *
RMSD bond angle	0.030 *
Refinement software	PROLSQ

Data quality characteristics

	Overall
High resolution limit [Å]	2.060 *
Total number of observations	75552 *
Completeness [%]	0.1 *

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	unknown *	7 *	12-15 *	Poulos, T.L., (1982) J. Biol. Chem., 257, 10427. *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1		50 (mM)
2	1	1		250 (250)
3	1	1	dithiothreitol	50 (mM)
4	1	2	ammonium sulphate	66-70 (%sat)