Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

1PG5

CRYSTAL STRUCTURE OF THE UNLIGATED (T-STATE) ASPARTATE TRANSCARBAMOYLASE FROM THE EXTREMELY THERMOPHILIC ARCHAEON SULFOLOBUS ACIDOCALDARIUS

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsELETTRA BEAMLINE 5.2R
Synchrotron siteELETTRA
Beamline5.2R
Temperature [K]100
Detector technologyCCD
Collection date2002-02-22
DetectorMARRESEARCH
Wavelength(s)1.00
Spacegroup nameP 63 2 2
Unit cell lengths132.853, 132.853, 140.279
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution20.000 - 2.600
R-factor0.19521
Rwork0.193
R-free0.23862
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)8at1
RMSD bond length0.025
RMSD bond angle2.452
Data reduction softwareDENZO
Data scaling softwareSCALEPACK
Phasing softwareAMoRE
Refinement softwareREFMAC (5.1.24)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.640
High resolution limit [Å]2.5902.590
Number of reflections23141
Completeness [%]99.798.9
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP4298ammonium sulfate, sodium acetate, pH 4, VAPOR DIFFUSION, HANGING DROP, temperature 298.0K

222624

PDB entries from 2024-07-17

PDB statisticsPDBj update infoContact PDBjnumon