1PBK
HOMOLOGOUS DOMAIN OF HUMAN FKBP25
Experimental procedure
Detector technology | AREA DETECTOR |
Collection date | 1993-12-28 |
Detector | XUONG-HAMLIN MULTIWIRE |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 86.000, 86.000, 55.600 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 8.000 - 2.500 |
R-factor | 0.191 * |
Rwork | 0.185 |
R-free | 0.24400 * |
RMSD bond length | 0.011 |
RMSD bond angle | 2.880 * |
Data reduction software | DENZO |
Phasing software | X-PLOR (3.1) |
Refinement software | X-PLOR (3.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 * | |
High resolution limit [Å] | 2.500 | 2.500 * |
Rmerge | 0.065 | 0.285 * |
Total number of observations | 24730 * | |
Number of reflections | 7520 * | |
Completeness [%] | 98.1 * | 99.4 * |
Redundancy | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 8.1 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 30-35 (%(w/v)) | |
2 | 1 | reservoir | HEPES | 100 (mM) |