1PA2
ARABIDOPSIS THALIANA PEROXIDASE A2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX II BEAMLINE I711 |
Synchrotron site | MAX II |
Beamline | I711 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 1998-05-01 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 46.156, 74.597, 80.446 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 99.000 - 1.450 |
R-factor | 0.1398 * |
R-free | 0.18910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1atj |
RMSD bond length | 0.009 |
RMSD bond angle | 0.024 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | SHELXL |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.000 | 1.510 |
High resolution limit [Å] | 1.450 | 1.450 |
Rmerge | 0.058 * | 0.243 * |
Total number of observations | 280003 * | |
Number of reflections | 49745 | 5403 * |
<I/σ(I)> | 19.1 | 8.4 |
Completeness [%] | 99.0 | 99 |
Redundancy | 5.6 | 4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 6.5 | pH 6.5 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 0.98 (mg/ml) | |
2 | 1 | drop | magnesium acetate | 0.1 (M) | |
3 | 1 | drop | cacodylate | 0.5 (M) | |
4 | 1 | drop | PEG8000 | 10 (%(w/v)) | |
5 | 1 | reservoir | magnesium acetate | 0.2 (M) | |
6 | 1 | reservoir | cacodylate | 0.1 (M) | |
7 | 1 | reservoir | PEG8000 | 20 (%(w/v)) |