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1P59

Structure of a non-covalent Endonuclease III-DNA Complex

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2002-11-20
DetectorRIGAKU RAXIS IV
Wavelength(s)1.5418
Spacegroup nameP 21 21 2
Unit cell lengths66.321, 105.896, 41.518
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution30.000

*

- 2.500
R-factor0.214
Rwork0.214
R-free0.26900
Structure solution methodFOURIER SYNTHESIS
Starting model (for MR)1orn
RMSD bond length0.008
RMSD bond angle19.100

*

Data scaling softwareSCALEPACK
Phasing softwareCNS
Refinement softwareCNS (1.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.590
High resolution limit [Å]2.5002.500
Rmerge0.0560.271
Number of reflections17421
<I/σ(I)>19.63.7
Completeness [%]89.083.1
Redundancy3.3

*

2.7
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.5298PEG 8000, TRIS, BME, pH 8.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K
Crystallization Reagents
IDcrystal IDsolution IDreagent nameconcentrationdetails
111PEG 8000
211TRIS
311BME
412PEG 8000
512TRIS
612BME
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11reservoirTris100 (mM)pH8.5
21reservoirPEG800020-25 (%(w/v))
31reservoirbeta-mercaptoethanol5 (mM)

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