1OY1
X-Ray Structure Of ElbB From E. Coli. Northeast Structural Genomics Research Consortium (Nesg) Target Er105
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | NSLS BEAMLINE X12C |
Synchrotron site | NSLS |
Beamline | X12C |
Temperature [K] | 90 |
Detector technology | CCD |
Collection date | 2002-11-22 |
Detector | BRANDEIS - B4 |
Wavelength(s) | 0.97900, 0.78911, 0.9200 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 99.108, 105.522, 165.102 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.000 - 2.950 |
Rwork | 0.216 |
R-free | 0.26500 |
Structure solution method | MAD |
RMSD bond length | 0.007 |
RMSD bond angle | 1.366 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | CNS |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 3.010 |
High resolution limit [Å] | 2.950 | 2.950 |
Number of reflections | 18121 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | VAPOR DIFFUSION, HANGING DROP, 3.3 M SODIUM FORMATE, 12mM pyridoxal at 30C |