1OXY
CRYSTALLOGRAPHIC ANALYSIS OF OXYGENATED AND DEOXYGENATED STATES OF ARTHROPOD HEMOCYANIN SHOWS UNUSUAL DIFFERENCES
Experimental procedure
| Spacegroup name | H 3 2 |
| Unit cell lengths | 117.240, 117.240, 285.860 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 6.000 - 2.400 |
| R-factor | 0.171 |
| Rwork | 0.171 |
| RMSD bond length | 0.017 |
| RMSD bond angle | 3.527 |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | |
| Number of reflections | 32972 |
| Completeness [%] | 81.0 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 6.2 * |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | 0.5 (M) | ||
| 2 | 1 | 1 | Bis-Tris | 0.16 (M) | |
| 3 | 1 | 1 | Tris-glycine | 0.03 (M) | |
| 4 | 1 | 1 | 0.006 (M) | ||
| 5 | 1 | 1 | PEG8000 | 4 (%) |
