1OX3
crystal structure of mini-fibritin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ELLIOTT GX-20 |
Temperature [K] | 277.189 |
Detector technology | IMAGE PLATE |
Detector | MACSCIENCE |
Wavelength(s) | 1.5418 |
Spacegroup name | P 63 |
Unit cell lengths | 54.615, 54.615, 107.848 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.360 - 2.000 |
R-factor | 0.209 |
Rwork | 0.209 |
R-free | 0.22100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1aa0.pdb |
RMSD bond length | 0.009 |
RMSD bond angle | 1.300 |
Data reduction software | MOSFLM |
Data scaling software | CCP4 ((SCALA)) |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 24.400 |
High resolution limit [Å] | 2.000 |
Number of reflections | 12329 |
<I/σ(I)> | 5.8 |
Completeness [%] | 99.7 |
Redundancy | 6.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 303 | PEG 6000, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 303K |