1OX3
crystal structure of mini-fibritin
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | ELLIOTT GX-20 |
| Temperature [K] | 277.189 |
| Detector technology | IMAGE PLATE |
| Detector | MACSCIENCE |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 63 |
| Unit cell lengths | 54.615, 54.615, 107.848 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 24.360 - 2.000 |
| R-factor | 0.209 |
| Rwork | 0.209 |
| R-free | 0.22100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1aa0.pdb |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.300 |
| Data reduction software | MOSFLM |
| Data scaling software | CCP4 ((SCALA)) |
| Phasing software | AMoRE |
| Refinement software | CNS (1.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 24.400 |
| High resolution limit [Å] | 2.000 |
| Number of reflections | 12329 |
| <I/σ(I)> | 5.8 |
| Completeness [%] | 99.7 |
| Redundancy | 6.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 303 | PEG 6000, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 303K |
