1OWM
DATA1:DNA photolyase / received X-rays dose 1.2 exp15 photons/mm2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44B2 |
Synchrotron site | SPring-8 |
Beamline | BL44B2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2002-01-29 |
Detector | MARRESEARCH |
Wavelength(s) | 1 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 89.329, 89.329, 133.403 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.970 - 2.300 |
R-factor | 0.214 |
Rwork | 0.211 |
R-free | 0.26300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.200 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.970 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Number of reflections | 24496 | |
Completeness [%] | 87.8 | 73.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | Ammonium Sulfate, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |