1OVV
CRYSTAL STRUCTURE OF FOUR-HELIX BUNDLE MODEL di-Co(II)-DF1-L13A (form II)
Experimental procedure
Experimental method | 1.200 |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2002-09-30 |
Detector | MARRESEARCH |
Wavelength(s) | 1.2000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 36.920, 80.050, 96.620 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 15.000 - 2.900 |
R-factor | 0.26943 |
Rwork | 0.267 |
R-free | 0.31979 |
Structure solution method | UNCONVENTIANAL METHOD USING THE GROUP-SUBGROUP RELATION |
RMSD bond length | 0.028 |
RMSD bond angle | 2.502 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Refinement software | REFMAC (5.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.300 | 3.060 |
High resolution limit [Å] | 2.900 | 2.900 |
Rmerge | 0.109 | 0.573 |
Number of reflections | 6492 | |
<I/σ(I)> | 11.2 | 3.1 |
Completeness [%] | 96.8 | 89 |
Redundancy | 5.7 | 5.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 298 | Peg 400, TRIS-HCl, pH 7.50, VAPOR DIFFUSION, HANGING DROP, temperature 298K |