1OVB
THE MECHANISM OF IRON UPTAKE BY TRANSFERRINS: THE STRUCTURE OF AN 18KD NII-DOMAIN FRAGMENT AT 2.3 ANGSTROMS RESOLUTION
Experimental procedure
Spacegroup name | P 31 |
Unit cell lengths | 41.500, 41.500, 81.900 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 7.000 - 2.300 |
R-factor | 0.195 |
Rwork | 0.195 |
RMSD bond length | 0.008 |
RMSD bond angle | 0.011 * |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 * |
Rmerge | 0.044 * |
Total number of observations | 13822 * |
Number of reflections | 6535 * |
Completeness [%] | 90.1 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.8 * | 4 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | protein | 40 (mg/ml) | |
2 | 1 | reservoir | MPD | 40 (%(v/v)) | |
3 | 1 | reservoir | Tris-HCl | 50 (mM) |