1OTE
E46Q MUTANT OF PHOTOACTIVE YELLOW PROTEIN, P65 AT 110K
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 14-BM-C |
Synchrotron site | APS |
Beamline | 14-BM-C |
Temperature [K] | 110 |
Detector technology | CCD |
Collection date | 2001-05-15 |
Detector | ADSC QUANTUM 4 |
Wavelength(s) | 0.9 |
Spacegroup name | P 65 |
Unit cell lengths | 40.018, 40.018, 117.610 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 20.000 - 1.400 |
R-factor | 0.185 |
Rwork | 0.182 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2phy |
RMSD bond length | 0.015 |
RMSD bond angle | 2.440 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | CNS |
Refinement software | SHELXL-97 |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 100.000 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.070 | 0.130 |
Number of reflections | 20725 | |
<I/σ(I)> | 22.3 | 13.2 |
Completeness [%] | 96.5 | 94.3 |
Redundancy | 24.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | PEG 2000, MES, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 110K |