1OO9
Orientation in Solution of MMP-3 Catalytic Domain and N-TIMP-1 from Residual Dipolar Couplings
Spectrometer
Experimental method: SOLUTION NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | DRX | 500 | |
| 2 | Varian | UNITYPLUS | 720 | |
| 3 | Bruker | DRX | 750 | |
| 4 | Varian | INOVA | 600 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 15N-separated NOESY; HNCA; HNCO; HN(CO)CA |
| 2 | 1 | 1 | HCCH-TOCSY; HCCH-COSY; |
| 3 | 2 | 3 | 15N-separated NOESY; HNCA; HNCO; HN(CO)CA |
| 4 | 2 | 4 | 15N-separated NOESY |
| 5 | 1 | 2 | 15N-separated NOESY |
| 6 | 2 | 5 | 15N-separated NOESY |
| 7 | 2 | 6 | coupled 15N-HSQC; coupled 13C-HSQC; Ha-coupled HNCA |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.6 | ambient | 310 |
| 2 | 6.7 | ambient | 307 |
Conformers
| Conformers Calculated Total Number | 25 |
| Conformers Submitted Total Number | 1 |
