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1OKQ

LAMININ ALPHA 2 CHAIN LG4-5 DOMAIN PAIR, CA1 SITE MUTANT

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU RUH3R
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2002-10-14
DetectorMARRESEARCH
Spacegroup nameC 2 2 21
Unit cell lengths70.110, 110.734, 123.835
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution20.000 - 2.800
R-factor0.22
Rwork0.220
R-free0.27000
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1dyk
RMSD bond length0.007
RMSD bond angle1.300

*

Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwareAMoRE
Refinement softwareCNS (1.1)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]20.0002.950
High resolution limit [Å]2.8002.800
Rmerge0.1010.230

*

Number of reflections11824
<I/σ(I)>15.67.3
Completeness [%]97.397.3
Redundancy6.56.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1unknown

*

7.5pH 7.50
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein12 (mg/ml)
21dropHEPES0.01 (M)pH7.5
31drop0.14 (M)
41drop10 (mM)
51reservoirPEG4000

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