1OH4
Structural and thermodynamic dissection of specific mannan recognition by a carbohydrate-binding module
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID14-1 |
Synchrotron site | ESRF |
Beamline | ID14-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Detector | ADSC CCD |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 31.790, 48.919, 96.421 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.220 - 1.350 |
R-factor | 0.14 |
Rwork | 0.138 |
R-free | 0.17000 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1of3 |
RMSD bond length | 0.017 |
RMSD bond angle | 1.853 |
Data reduction software | MOSFLM |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.24) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 1.420 | 1.420 |
High resolution limit [Å] | 1.350 | 1.350 |
Rmerge | 0.057 | 0.261 |
Number of reflections | 31455 | |
<I/σ(I)> | 17.5 | 2.9 |
Completeness [%] | 97.8 | 87.3 |
Redundancy | 4.7 | 2.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 4.6 | 1.5 M AMMONIUM SULFATE, 0.1 M SODIUM ACETATE PH 4.6 |