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1OFG

GLUCOSE-FRUCTOSE OXIDOREDUCTASE

Experimental procedure
Source typeROTATING ANODE
Source detailsRIGAKU
Temperature [K]277
Detector technologyIMAGE PLATE
Collection date1996-04
DetectorRIGAKU
Spacegroup nameP 21 21 2
Unit cell lengths84.490, 283.690, 116.990
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution50.000 - 2.700
R-factor0.203

*

Rwork0.203
Structure solution methodMULTIPLE ISOMORPHOUS REPLACEMENT
RMSD bond length0.013
RMSD bond angle22.900

*

Data reduction softwareDENZO
Data scaling softwareCCP4
Refinement softwareTNT
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0002.870
High resolution limit [Å]2.7002.700
Rmerge0.0900.265
Total number of observations353200

*

Number of reflections715007701

*

Completeness [%]91.060
Redundancy4.82
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1Vapor diffusion, hanging drop

*

5.5pH 5.5
Crystallization Reagents in Literatures
IDcrystal IDsolutionreagent nameconcentration (unit)details
11dropprotein10 (mg/ml)
21reservoirPEG60005-15 (%(w/v))
31reservoirsuccinic acid/KOH0.2 (M)or 0.2 M citric acid/KOH

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PDB entries from 2024-11-06

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