1OEJ
YodA from Escherichia coli crystallised with no added ions
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SRS BEAMLINE PX9.5 |
| Synchrotron site | SRS |
| Beamline | PX9.5 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2001-02-15 |
| Detector | MARRESEARCH |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 40.348, 64.558, 41.499 |
| Unit cell angles | 90.00, 117.83, 90.00 |
Refinement procedure
| Resolution | 36.760 - 1.800 * |
| R-factor | 0.18371 |
| Rwork | 0.180 |
| R-free | 0.25200 * |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1oee |
| RMSD bond length | 0.018 * |
| RMSD bond angle | 1.467 * |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | REFMAC |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 14.920 | 1.910 |
| High resolution limit [Å] | 1.810 | 1.810 |
| Rmerge | 0.060 | 0.588 |
| Number of reflections | 6027 | |
| <I/σ(I)> | 10.5 | 1.6 |
| Completeness [%] | 74.5 | 69.7 |
| Redundancy | 1.6 | 1.6 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | other * | 6.5 | David, G., (2002) Acta Cryst., D58, 1243. * |
