1OCW
Free conformation Ab2 of the IgE SPE-7
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2002-08-15 |
| Detector | MARRESEARCH |
| Spacegroup name | I 4 |
| Unit cell lengths | 79.545, 79.545, 67.703 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 28.170 - 2.000 |
| R-factor | 0.252 * |
| R-free | 0.21000 * |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1oaq |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Phasing software | AMoRE |
| Refinement software | SHELXL-97 |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 28.170 |
| High resolution limit [Å] | 2.010 |
| Rmerge | 0.051 |
| Number of reflections | 13952 |
| Completeness [%] | 94.4 |
| Redundancy | 9.9 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | 5 | 0.1M HEPES, PH7.5, 70% MPD, pH 5.00 |
