1OBP
ODORANT-BINDING PROTEIN FROM BOVINE NASAL MUCOSA
Experimental procedure
| Source type | ROTATING ANODE |
| Temperature [K] | 289 |
| Detector technology | IMAGE PLATE |
| Collection date | 1995-05-26 |
| Detector | MAR scanner 180 mm plate |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 55.900, 65.500, 42.700 |
| Unit cell angles | 90.00, 98.80, 90.00 |
Refinement procedure
| Resolution | 6.000 - 2.000 |
| R-factor | 0.164 |
| Rwork | 0.164 |
| R-free | 0.24700 |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.530 |
| Data reduction software | DENZO |
| Phasing software | X-PLOR (3.1) |
| Refinement software | X-PLOR (3.1) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 2.000 |
| Rmerge | 0.045 |
| Number of reflections | 20232 |
| Completeness [%] | 94.6 |
| Redundancy | 3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 5.7 | pH 5.7 |
Crystallization Reagents in Literatures
| ID | crystal ID | solution | reagent name | concentration (unit) | details |
| 1 | 1 | 1 | ethanol | 35-45 (%) |
