1OAR
Fv IgE SPE-7 in complex with Alizarin Red
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-11-15 |
Detector | MARRESEARCH |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.917, 78.882, 169.036 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.710 - 2.200 * |
Rwork | 0.205 |
R-free | 0.24300 * |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1ANQ |
RMSD bond length | 0.007 * |
RMSD bond angle | 1.300 * |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | AMoRE |
Refinement software | REFMAC (5.1.19) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.800 | |
High resolution limit [Å] | 2.200 * | |
Rmerge | 0.067 | 0.325 * |
Number of reflections | 52239 * | |
Completeness [%] | 99.6 | 99.4 * |
Redundancy | 13.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 5.5 * | 21% PEG 8K, 0.1M NA CACODYLATE, 0.2M NA ACETATE PH5.5, pH 5.00 |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | PEG8000 | 21 (%) | |
2 | 1 | reservoir | sodium cacodylate | 0.1 (M) | |
3 | 1 | reservoir | sodium acetate | 0.2 (M) | pH5.5 |