1OAK

CRYSTAL STRUCTURE OF THE VON WILLEBRAND FACTOR (VWF) A1 DOMAIN IN COMPLEX WITH THE FUNCTION BLOCKING NMC-4 FAB

Experimental procedure

Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL7-1
Synchrotron site	SSRL
Beamline	BL7-1
Temperature [K]	90
Detector technology	IMAGE PLATE
Collection date	1995-06
Detector	MARRESEARCH
Spacegroup name	C 1 2 1
Unit cell lengths	208.200, 61.900, 72.900
Unit cell angles	90.00, 108.60, 90.00

Refinement procedure

Resolution	50.000 - 2.200
R-factor	0.201
Rwork	0.201
R-free	0.27400
Structure solution method	MOLECULAR REPLACEMENT AND MULTIPLE ISOMORPHOUS REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.400
Data reduction software	DENZO
Data scaling software	SCALEPACK
Phasing software	PHASES
Refinement software	X-PLOR

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	50.000	2.300
High resolution limit [Å]	2.200	2.200
Rmerge		0.184
Number of reflections	44346
<I/σ(I)>	18.1	6.4
Completeness [%]	99.0	98.5
Redundancy	3.4	3.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		8		pH 8