1OA9
Structure of Melanocarpus albomyces endoglucanase
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | EMBL/DESY, HAMBURG BEAMLINE X11 |
Synchrotron site | EMBL/DESY, HAMBURG |
Beamline | X11 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2001-07-15 |
Detector | MARRESEARCH |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 47.304, 47.304, 177.328 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 * - 2.000 |
R-factor | 0.215 |
Rwork | 0.215 |
R-free | 0.27600 * |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3eng |
RMSD bond length | 0.006 |
RMSD bond angle | 1.410 * |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | AMoRE |
Refinement software | CNS (1.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.060 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.079 | 0.290 |
Total number of observations | 296601 * | |
Number of reflections | 13270 * | |
<I/σ(I)> | 8 | 1.5 |
Completeness [%] | 91.2 | 87.4 |
Redundancy | 22.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 4.6 | Hirvonen, M., (2002) Acta Cryst., D58, 336. * |