1O9S
Crystal structure of a ternary complex of the human histone methyltransferase SET7/9
Experimental procedure
| 実験手法 | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU RU200 |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Detector | RIGAKU IMAGE PLATE |
| Spacegroup name | P 1 21 1 |
| 格子定数 [Å] | 52.690, 75.438, 69.099 |
| 格子定数 [度] | 90.00, 94.16, 90.00 |
精密化法
| 残基 | 20.000 - 1.750 |
| R因子 | 0.206 |
| Rwork | 0.205 |
| R-free | 0.22200 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 1h3i |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | AMoRE |
| Refinement software | REFMAC |
Quality characteristics
| Overall | |
| 分解能 [Å] (低) | 20.000 |
| 分解能 [Å] (高) | 1.750 |
| 独立反射数 | 54703 |
| <I/σ(I)> | 47.2 |
| 完全性 [%] | 89.9 |
| 冗長性 | 22 |
結晶化条件
| 結晶ID | 方法 | pH | 温度 | 溶液条件 |
| 1 | 7.8 | pH 7.80 |
