1O1S
Structure of FPT bound to isoprenoid analog 3b
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 100 |
| Detector technology | IMAGE PLATE |
| Collection date | 2000-03-15 |
| Detector | RIGAKU RAXIS IV |
| Spacegroup name | P 61 |
| Unit cell lengths | 171.830, 171.830, 69.090 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 8.000 - 2.300 |
| R-factor | 0.19 |
| Rwork | 0.190 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | X-PLOR |
| Refinement software | X-PLOR |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 50.000 | 2.330 |
| High resolution limit [Å] | 2.300 * | 2.250 |
| Rmerge | 0.038 | 0.354 |
| Number of reflections | 54254 | |
| <I/σ(I)> | 30.9 | |
| Completeness [%] | 97.5 | 95.6 |
| Redundancy | 3.4 | 3.4 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | unknown * | 5.7 | 298 | PEG 4000, Sodium Acetate, KCl, pH 5.7, hanging drop, temperature 298.0K |
