1O1S
Structure of FPT bound to isoprenoid analog 3b
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2000-03-15 |
Detector | RIGAKU RAXIS IV |
Spacegroup name | P 61 |
Unit cell lengths | 171.830, 171.830, 69.090 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 8.000 - 2.300 |
R-factor | 0.19 |
Rwork | 0.190 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | X-PLOR |
Refinement software | X-PLOR |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.330 |
High resolution limit [Å] | 2.300 * | 2.250 |
Rmerge | 0.038 | 0.354 |
Number of reflections | 54254 | |
<I/σ(I)> | 30.9 | |
Completeness [%] | 97.5 | 95.6 |
Redundancy | 3.4 | 3.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | unknown * | 5.7 | 298 | PEG 4000, Sodium Acetate, KCl, pH 5.7, hanging drop, temperature 298.0K |